Tuesday, 23 August 2016

Microemulsification-Based Method: Coupling with Separation Technique

Point-of-use devices represent currently a key field in quantitative analytical sciences. These platforms are low-cost, fast, portable, and simple to use eliminating the necessity for qualified operators. Rapid tests enable in-situ measurements presenting substantial social and economic implications at industry, environment, and medicine. One potential output to perform point-of-use analyses is the accomplishment of the tests in solution with naked eye detection using disposable systems. It allows the determination of different analytes from the use of modified nanomaterial. Naked eye methods bypasses the use of instrumental readers, an essential feature for in-situ technologies. Furthermore, the analyses in solution surpass precisionrelated downsides when making the tests on substrates such as paper.

Microemulsification-Based Method

In this case, the diverse paper substrates that are employed to fabricate the devices affect the flow rates and interactions with analytes.This paper reports further investigations and application of the microemulsification-based method (MEC), a point-of-use platform that was recently proposed by these authors. It relies on solutionbased- detection with naked eyes. In contrast with colorimetric tools, MEC response depends on colloid thermodynamics by relying on effect of analyte on the entropy of emulsions or Winsor systems. It changes the formation ofthermodynamically stable dispersions, the microemulsions (MEs). The minimum volume fraction of amphiphile (AP) needed to get MEs (ΦME) for a fixed water-oil ratio expressed the analytical signal of the method.

The generation of nanodroplets in MEs (transparent) allows the naked eye detection of ΦME by monitoring the change of turbidity from the emulsions or Winsor systems (cloudy). This cloudy-to-transparent conversion acts like a turning point in titrations, ensuring the visual measurement of ME and, therefore, not only screening analyses (positive/negative data) as the most of naked eye colorimetry platforms as well as precise quantitative analyses. The response in colorimetry changes with the intensity of colour or tonality. Herein, subjective uncertainties by personal and surrounding conditions are observed.

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